Chromatography yamadzimadzi Chitsulo chosapanga dzimbiri capillary chromasir
Pali mitundu itatu ya zitsulo zosapanga dzimbiri capillary: Traline capillary, Ribend capillary ndi Supline capillary. Ma capillary onse amatenga 316L chitsulo chosapanga dzimbiri ngati chuma, chokhala ndi 1.58mm (1/16inch) m'mimba mwake mbali zonse ziwiri, 0.79mm (1/32inch) awiri akunja pakati. Traline zitsulo zosapanga dzimbiri capillary amakonda kukhala pliant, ndipo amakana 1200bar ndi acid-base bwino. Mapeto onse a Ribend capillary adapangidwa kuti akhale opendekera, omwe amalepheretsa kudulidwa. Imakana 1200bar ndi acid-base bwino. Poyerekeza ndi mndandanda wa Traline, Ribend amakhala ndi moyo wautali, wokhala ndi vuto lomwe lingagwiritsidwe ntchito pophatikiza zitsulo zazifupi. Mapeto onse a Supline capillary adapangidwa ndi setifiketi ya "ng'oma" mawonekedwe; ndiye capillary yodzaza ndi gasket yosindikiza, pambuyo polimbitsa chala, kusindikiza kawiri kwa ndege ndi mbali kumatha kutheka. Capillary imakhala yopindika, yomwe imalepheretsa kusweka. Itha kukana kuposa 1200bar, komanso acid-base. Ma capillary ndi oyenera amatha kupatulidwa ndikusinthidwa okha, ndi moyo wake mpaka nthawi 150 (za jekete lolowera ndi chipangizo). Poyerekeza ndi mndandanda wa Traline ndi Ribend, mndandanda wa Supline ukhoza kukwanitsa kusindikiza kawiri, kugwiritsa ntchito mitundu yonse ya mizati ya chromatographic, ndikuchepetsa kulumikizidwa kwakufa kwa capillary.
Zitsulo zosapanga dzimbiri za capillary zolimba zala ndizosavuta kugwiritsa ntchito ndikuyika mwachangu popanda zida zilizonse, ngakhale zimayikidwa pamizere yapamwamba kwambiri ya chromatographic ndikusintha ma valves. Kuyika kwa capillary kumagwirizana ndi mizati yodziwika bwino ya chromatographic ndi mavavu, ndikukana kukakamiza kwadongosolo mpaka 400 bar.
1. Capillary imapangidwa ndi machubu a 316L osapanga dzimbiri, omwe amatsukidwa ndi kutentha kwambiri.
2. Kukana kwabwino kwa 1200 bar ndi koyenera kwa mapulogalamu ambiri okhazikika.
3. Malo osalala mu chubu mkati kuti muchepetse kupsyinjika.
4. 1/16 mainchesi pa malekezero onse awiri, zoyenera zambiri zamadzimadzi chromatograph.
5. Kuyika chala kumbali zonse ziwiri (kusagwirizana ndi mipiringidzo ya 400), koyenera machitidwe ambiri a LC.
6. Imapezeka mu 150mm/250mm/350mm/550mm kutalika kwa chubu.
7. Kuyika kwachala ndikwaulere kusuntha ndipo kutha kugwiritsa ntchito ma chromatograph osiyanasiyana.